Decree of the Ministry of Agriculture No. 16 / 2000 Coll.
Decree of the Ministry of Agriculture amending Decree of the Ministry of Agriculture No. 222 / 1996 Coll., laying down methods of sampling, methods of analysis of feed, additives and premixtures and method of storage of samples subject to destruction
Valid
Effective from 11.04.2000
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16
DECLARATION
Ministry of Agriculture
of 26 January 2000
amending Decree No 222 / 1996 of the Ministry of Agriculture Coll., laying down the methods of sampling, the methods of analysis of feed, additives and premixtures and the method of storage of samples subject to destruction
The Ministry of Agriculture provides according to § 4 (7) and § 17 (6) of Act No. 91 / 1996 Coll., on feedingstuffs:
Decree No 222 / 1996 Coll., laying down the methods of sampling, the methods of analysis of feed, feed additives and premixtures and the method of storage of samples subject to destruction, shall be amended as follows:
1. in Article 1 (2), including footnote (1a):
"(2) The sampling of feed, feed additives and premixtures shall include the taking of incremental samples for the purposes of the compilation of the aggregate and final samples, the taking of incremental samples for the purpose of determining the working accuracy of the mixing device and the assessment of the homogeneity of the additives and amino acids in premixtures and feedingstuffs using premixtures (hereinafter referred to as" homogeneity ') and the method of marking and storage of final and, where appropriate, incremental samples, including the production of a report on their collection. This provision shall not apply to sampling for the determination of pesticide residues and the presence of micro-organisms, which shall be carried out under specific legislation. (1a)
(1a) Decree No 294 / 1997 Coll., on microbiological requirements for foodstuffs, their method of control and evaluation, as amended by Decree No 91 / 1999 Coll. '
2. In Article 2, at the end of paragraph 4, the dot is deleted and the words "or for the assessment of the working accuracy of the mixing equipment are added."
3. In Article 2, the following sentence is added at the beginning of paragraph 6: "The quantity of feed, feed additive or premixture showing consistency by its external arrangement, labelling and local storage shall be considered as the sampled lot. '
4. In Article 2, the following paragraph 7 is added:
"(7) When taking incremental samples to assess the working accuracy of the mixing device, 10 incremental samples shall be taken from the content of the mixing device considered as set out in Annex 16. ';
5. In Article 3 (2), the words "or to assess the working accuracy of mixing equipment 'shall be inserted after the words" using the prefix'.
6. In Article 3, the following paragraph 4 is inserted after paragraph 3:
"(4) When sampling to assess the working accuracy of the agitators, the incremental sample taken from the agitators shall always constitute one aggregate sample which is considered to be the final sample at the same time. ';
Paragraph 4 shall become paragraph 5.
7. Paragraph 4 (1) reads as follows:
"(1) At least three final samples shall be taken directly or after reduction from the aggregate sample, which shall constitute the quantity of the aggregate sample to be tested; the minimum weight of the final sample is given in column 2 of Annex 5. ';
8. In Article 4 (2), the words "and for the assessment of the working accuracy of the mixing device 'shall be inserted after the words" using the prefix'.
9. In Section 4, the following paragraph 4 is added:
"(4) Samples intended for laboratory testing shall be delivered without delay together with the sampling protocol to the laboratory concerned.
4) Article 17 of Act No. 91 / 1996 Coll., on Feed. '.
10. In Article 5, paragraphs 4 to 6 are added:
"(4) The provisions of paragraphs 1, 2 and 3 shall not apply to incremental samples taken to assess the homogeneity and working accuracy of the mixing equipment.
(5) When taking incremental samples for the assessment of homogeneity or the working accuracy of the mixing devices, the incremental samples, which are also final samples, shall be kept in clean, dry, moisture-free, airtight sealed packages. The packaging shall be sealed and marked with the following particulars:
(a) the name of the sampled feed, additive, premixture or, for samples, for the assessment of working accuracy by the type of mixing device verified;
(b) the commercial name and registered office of the legal person or the name and surname of the natural person who is the manufacturer of the feed, the additive and the premixture, for samples for the assessment of the working accuracy on the commercial name and address of the legal person or the name and surname of the natural person who is the owner of the mixing establishment;
(c) the name and surname of the natural person responsible for sampling.
(6) When sampling feed, additives and premixtures intended for the testing of photolable substances, the final samples shall be kept in packages which prevent light access. ';
11. in Paragraph 6 (1):
"(1) A protocol shall be drawn up for each final sample of feed, feed additive and premixture to allow the accurate identification of each sampled lot in such a way that there is no confusion between the samples. The sampling protocol shall be attached to each final sample. For the purpose of assessing the homogeneity or working accuracy of the agitators, only one protocol shall be taken for all samples. ';
12. in Article 7, the following paragraph 3 is added:
"(3) Where a method for testing a given character is not listed in Annexes 7 to 14 and checking that character is necessary, another appropriate method may be used which corresponds to the achieved level of scientific and technical knowledge. The general conditions for using the test method are set out in Annex 15. ';
13. in Paragraph 9 (1):
"(1) After the completion of the tests, the test samples of feed, feed additives and premixtures shall be kept in accordance with the methods set out in Annex 8."
14. Paragraph 10 (3) reads:
"(3) The concentration of solutions shall be expressed either by weight or volume percentage, or expressed as a concentration of the substance (mol / l) or by weight (mg / l, mg / ml). ';
15.
(1) The chemical test of feed, feed additive or premixture results in an average value obtained from at least two analyses carried out on two samples, provided that the analytical result does not deviate by a value greater than the limit of repeatability / r / (hereinafter referred to as repeatability) set out in Annexes 9 and 10.
(2) Repeatability is a value that can be assumed to be less than or equal to the absolute value of the difference between the two test results obtained under repeatability conditions with 95% probability. Repeatability conditions are conditions where independent test results are obtained by the same method, on identical material, in the same laboratory, by the same worker, using the same equipment, within a short period of time.
(3) If the repeatability value is not stated, it shall be calculated in accordance with the procedure set out in point 8 of Annex No 15.
(4) The chemical test result shall be expressed in the units listed in Annexes 9 to 14. In determining the original moisture content of feed, feed additive or premixture, the results shall be converted into the original dry matter.
(5) Unless otherwise stated for the method, the results shall be expressed after rounding as follows:
for expressing content in mg / kg:
| pro obsah do 9,99 mg/kg | s přesností na 0,01 mg/kg |
| pro obsah od 10,0 do 99,9 mg/kg | s přesností na 0,1 mg/kg |
| pro obsah od 100 do 999 mg/kg | s přesností na 1 mg/kg |
| pro obsah od 1000 do 9999 mg/kg | s přesností na 10 mg/kg |
| pro obsah od 10000 do 99999 mg/kg | s přesností na 100 mg/kg |
| pro obsah nad 100 000 mg/kg | s přesností na 1000 mg/kg |
for expressing content in g / kg:
| pro obsah do 9,99 g/kg | s přesností na 0,01 g/kg |
| pro obsah od 10 g/kg do 99,9 g/kg | s přesností na 0,1 g/kg |
| pro obsah nad 100 g/kg | s přesností na 1 g/kg. |
(6) The limit of reproducibility / R / (hereinafter referred to as "reproducibility") is a value that can be assumed to be less than or equal to the absolute value of the difference between the two test results obtained under reproducibility conditions. Reproducibility conditions are conditions where independent test results are obtained by the same method, on indentic material in different laboratories, different workers using different equipment. Reproducibility does not include a sampling error.
(7) The reproducibility values for each test method are set out in Annexes 9, 10 and 17. If the reproducibility value is not determined, it shall be calculated in accordance with the procedure set out in point 8 of Annex No 15. ';
16.
The test of homogeneity (2) of the additives and amino acids in the premixture or feed batch using premixtures shall be carried out using the additive or the added amino acid. In assessing the working accuracy of the agitator (2), an additive shall be used which shows the lowest value of repeatability and reproducibility for the content verified in the laboratory. ';
17. In Annex 2, the title of the table, including the explanatory note at the end of the Annex, reads:
"Minimum number of incremental samples *)
Materials are feed, feed additives and premixtures.
*) Not applicable to the sampled lot if the number of packages or weight or volume is lower than that shown in the table. ';
18. In Annex No 2, point 1, the words "Solid feedingstuffs' are replaced by the words" Solid materials'.
19. In Annex 2, point 2, the words "Solid feedingstuffs packed in packs: 'are replaced by the words" Fixed materials packed in packages:';
20. In Annex 2, point 3, the words "Liquid and semi-liquid feed: 'are replaced by the words" Liquid and semi-liquid materials:';
21. In Annex 3, the title of the table, including the explanatory note at the end of the Annex, reads:
"Minimum weight of aggregate sample *)
*) Not applicable to the sampled lot if the number of packages or weight or volume is lower than that shown in the table. ';
22. Annex 5 reads as follows:
"Annex No 5 to Decree No 222 / 1996 Coll.
Minimum weight of final sample *)
| Druh a rozsah partie | Minimální hmotnost konečného vzorku |
|---|---|
| 1 | 2 |
| 1. Pevná krmiva | 0,5 kg |
| 2. Tekutá a polotekutá krmiva | 0,5 l |
| 3. Doplňkové látky | 0,05 kg |
| 4. Premixy | 0,25 kg. |
*) Not applicable to the sampled lot if the number of packages or weight or volume is lower than that shown in the table. ';
23. The heading of Annex 6 reads as follows:
"Sampling procedure for feed, feed additives and premixtures'.
24. The first sentence of point 1 of Annex 6 shall read as follows: "Partial samples with the exception of incremental samples for the determination of the presence and content of undesirable substances, prohibited substances and products, as well as subsamples for the determination of homogeneity and assessment of the working accuracy of the mixing devices shall be taken at random to cover the whole of the sampled lot. '
25. In Annex 6, the following points 5 and 6 are inserted after point 4:
"5. Partial samples for the assessment of the homogeneity of the lot shall be taken from randomly selected packaging or, in the case of bulk feed, from randomly selected sites which are evenly distributed across the sampled lot. The number of incremental samples taken from the lot is given in Annex 14.
6. The incremental samples to assess the working accuracy of the mixing device shall be taken in such a way that their collection is evenly distributed over the entire area of the mixing device space or, when sampled outside the mixing compartment, evenly distributed according to the number of packaging or weight sampled. ';
26. In Annex No 7, point 1.2, the following sentence is added at the end of the second paragraph: "This provision shall not apply to final samples to assess the content of undesirable substances, homogeneity and working accuracy of the mixing device. '.
27. In Annex No 7, the following points 1.6. and 1.7 are inserted after point 1.5.:
"1.6. The final samples for the assessment of the content of undesirable substances shall be assessed in advance in a sensory manner, any physical and special tests carried out, and the final sample shall be adjusted as a whole so that the particles fall through a wire sieve with a mesh size of 1 mm, and then mix perfectly so that the lashes required for each test are homogeneous and represent the final sample. For each test, the retractions shall be prepared from the sample thus modified.
1.7. The final samples for the assessment of homogeneity and for the assessment of the working accuracy of the mixing device shall first be adjusted as a whole so that the particles fall through a wire sieve with a mesh size of 1 mm and then mix perfectly so that the binders for each test are homogeneous and represent the final sample. The following shall be prepared from the samples so prepared:
28. Annex 9 reads as follows:
"Annex No 9 to Decree No 222 / 1996 Coll.
Procedures for laboratory testing of feed, feed additives and premixtures
List of procedures for chemical testing of feed
| Název postupu | Označení postupu | |
| 1. | Vlhkost, těkavé látky | |
| 1.1. | Stanovení obsahu vlhkosti v krmivech | -A- |
| 1.2. | Stanovení obsahu vlhkosti a těkavých látek v tucích | -A- |
| 1.3. | Stanovení obsahu vlhkosti a těkavých látek v olejnatých semenech | -A- |
| 1.4. | Stanovení obsahu vlhkosti | -B- |
| 1.5. | Stanovení obsahu vlhkosti v olejích a tucích | -B- |
| 2. | Dusíkaté sloučeniny | |
| 2.1. | Stanovení obsahu dusíkatých látek | -A- -B- |
| 2.2. | Stanovení obsahu dusíkatých látek rozpustných působením roztoku pepsinu v kyselině chlorovodíkové | -A- -B- |
| 2.3. | Stanovení obsahu bílkovin | -A- -B- |
| 2.4. | Stanovení obsahu aminokyselin | -B- |
| 2.5. | Stanovení obsahu močoviny | -A- -B- |
| 2.6. | Stanovení obsahu amoniaku v rybích moučkách | -A- -B- |
| 2.7. | Stanovení obsahu těkavých dusíkatých látek | -A- -B- |
| 2.8. | Stanovení aktivity ureázy v sóji a jejích produktech | -A- -B- |
| 2.9. | Ureázový test | -A- |
| 2.10. | Stanovení obsahu biuretu | -A- |
| 2.11. | Stanovení obsahu hydroxyanalogu methioninu | -A- |
| 2.12. | Stanovení obsahu dusíkatých látek rozpustných působením pepsinu | -B- |
| 2.13. | Stanovení aktivity pepsinu | -B- |
| 2.14. | Stanovení obsahu methioninu | -A- |
| 2.15. | Stanovení obsahu tryptofanu | -A- -B- |
| 3. | Tuk | |
| 3.1. | Stanovení obsahu tuku | -A- |
| 3.2. | Stanovení obsahu tuku v olejnatých semenech | -A- |
| 3.3. | Stanovení čísla kyselosti tuku | -A- |
| 3.4. | Stanovení obsahu lecitinu | -A- |
| 3.5. | Stanovení obsahu nerozpustných nečistot v tucích a olejích | -A- |
| 3.6. | Stanovení obsahu nezmýdelnitelných látek v tucích a olejích | -A- |
| 3.7. | Stanovení peroxidového čísla | -A- |
| 3.8. | Stanovení obsahu oleje a tuku | -B- |
| 4. | Polysacharidy | |
| 4.1. | Stanovení obsahu vlákniny | -A- -B- |
| 5. | Bezdusíkaté látky výtažkové | |
| 5.1. | Stanovení obsahu škrobu | -A- -B- |
| 5.2. | Stanovení obsahu škrobu - pankreatický postup | -B- |
| 5.3. | Stanovení obsahu cukrů | -A- -B- |
| 5.4. | Stanovení obsahu laktosy | -A- -B- |
| 5.5. | Stanovení obsahu bezdusíkatých látek výtažkových výpočtem | -A- |
| 5.6. | Stanovení obsahu cukrů polarizací | -A- -B- |
| 5.7. | Stanovení obsahu redukujících látek v cukru a melase | -A- |
| 6. | Popel | |
| 6.1. | Stanovení obsahu popele | -A- -B- |
| 6.2. | Stanovení obsahu popele v tucích | -A- |
| 6.3. | Stanovení obsahu nerozpustného podílu popele v kyselině | |
| chlorovodíkové | -A- -B- | |
| 6.4. | Stanovení obsahu popele nerozpustného v kyselině chlorovodíkové | -B- |
| 7. | Makroprvky | |
| 7.1. | Stanovení obsahu fosforu | -A- -B- |
| 7.2. | Stanovení obsahu vápníku | -A- -B- |
| 7.3. | Stanovení obsahu hořčíku | -A- -B- |
| 7.4. | Stanovení obsahu draslíku | -A- -B- |
| 7.5. | Stanovení obsahu sodíku | -A- -B- |
| 7.6. | Stanovení obsahu ve vodě rozpustných chloridů | -A- -B- |
| 7.7. | Stanovení obsahu celkových uhličitanů | -A- -B- |
| 7.8. | Stanovení obsahu oxidů křemíku, hliníku, vápníku a hořčíku (ve vápencích) | -A- |
| 7.9. | Stanovení celkového obsahu síry | -A- -B- |
| 7.10. | Stanovení obsahu vápníku | -B- |
| 8. | Mikroprvky | |
| 8.1. | Stanovení obsahů mědi, železa, manganu a zinku | -A- |
| 8.2. | Stanovení obsahu vápníku, mědi, železa, hořčíku, manganu, draslíku, sodíku a zinku | -B- |
| 8.3. | Stanovení obsahu železa, mědi, manganu a zinku | -B- |
| 9. | Kyselost | |
| 9.1. | Stanovení volné, vázané a celkové kyselosti vodního výluhu | -A- |
| 9.2. | Stanovení kyselosti vodního výluhu v mléčných krmných směsích | -A- |
| 10. | Nežádoucí látky | |
| 10.1. | Stanovení obsahu kyanovodíku | -B- |
| 10.2. | Stanovení obsahu hořčičného oleje vyjádřeného jako allylisothiokyanát | -B- |
| 10.3. | Stanovení obsahu theobrominu | -B- |
| 10.4. | Stanovení obsahu glukosinolátů v řepce | -A- -B- |
| 10.5. | Stanovení obsahu 5-vinyl-2-thiooxazolidonu | -A- -B- |
| 10.6. | Stanovení obsahu kyseliny erukové | -A- |
| 10.7. | Stanovení obsahu olova a kadmia | -A- |
| 10.8. | Stanovení obsahu ricinových slupek | -A- -B- |
| 10.9. | Stanovení obsahu fluoru | -B- |
| 10.10. | Stanovení obsahu rezidují organochlorových a organofosfátových pesticidů | -B- |
| 10.11. | Stanovení obsahu hexachlorbenzenu | -B- |
| 10.12. | Stanovení obsahu dusitanů | -B- |
| 10.13. | Stanovení obsahu rtuti | -A- |
| 10.14. | Stanovení obsahu aflatoxinu B1 | -B- |
| 10.15. | Stanovení obsahu arsenu | -B- |
| 10.16. | Stanovení obsahu gossypolu | -B- |
| 10.17. | Stanovení obsahu theobrominu | -A- |
| 11. | Zkoušení siláží | |
| 11.1. | Zkoušení jakosti siláží | -A- -B- |
1. Humidity, volatile substances
1.1. Determination of moisture content of feedingstuffs
Purpose, scope and principle
The procedure specifies the conditions for determining moisture content of feedingstuffs, premixtures and additives. The procedure is applicable for determining the moisture content of all types of feed, premixtures and additives with the exception of milk and milk products and oilseeds.
The moisture content shall be determined by weight as the reduction after drying of the sample at (103 ± 2) ° C, in the case of wet or separately named feedingstuffs after drying at 50 to 60 ° C under the prescribed conditions. In special cases, the moisture content shall be determined by drying at a reduced pressure at 80 ° C.
Repeatability
The difference between two parallel determinations carried out on the same sample shall not exceed 0,2% for all moisture content.
Reproducibility
The difference between the two test results of the same sample carried out in two laboratories shall not exceed the moisture content:
| do 15 % | 0,3 % |
| nad 15 % | 5 % relat. |
1.2. Determination of moisture and volatile matter content in fats
Purpose, scope and principle
The procedure determines the conditions for determining moisture and volatile substances in fats.
The moisture and volatile matter content is evaporated by drying at (103 ± 2) ° C and the weight loss is determined in a drastic manner.
Repeatability
The difference between two parallel determinations carried out on the same sample shall not exceed:
| do 2 % | 10 % relat. |
| nad 2 % | 0,2 % abs. |
Reproducibility
Not fixed.
1.3. Determination of moisture and volatile matter content of oilseeds
Purpose, scope and principle
The procedure determines the conditions for determining the moisture and volatile matter content of oilseeds. Determination of moisture content and volatile substances shall be made either from the material as it was obtained (pure seeds and impurities) or, if required, from the pure seeds themselves by drying at a temperature (103 ± 2) ° C in a drying room at atmospheric pressure to constant weight, in a dryness.
Repeatability
The difference between two parallel determinations carried out on the same sample shall not exceed 0,2% for all moisture content.
Reproducibility
Not fixed.
1.4. Determination of moisture content
Purpose, scope principle
The method makes it possible to determine the moisture content of feedingstuffs. In addition to the use for dairy products, it is suitable for most feedingstuffs, minerals, compound feed with predominantly mineral components and selected oil seeds and fruits. Determination of moisture content of oilseeds and fruits shall be governed by other legislation.
The moisture content shall be determined by weight as weight loss after drying the feed sample under the prescribed conditions. In case of higher moisture content of feed, pre-drying is necessary.
Repeatability
The difference between two parallel determinations carried out on the same sample shall not exceed 0,2% for all moisture content.
Reproducibility
Not fixed.
1.5. Determination of moisture content of oils and fats
Purpose, scope principle
The method allows the determination of water and volatile substances in animal and vegetable fats and oils.
The sample is dried to constant weight at 103 ° C. Weight loss is determined by weighing.
Repeatability
The difference between two parallel determinations carried out on the same sample shall not exceed 0,05% for all moisture content.
Reproducibility
Not fixed.
2. Nitrogen compounds
2.1. Determination of nitrogen content
Purpose, scope and principle
The procedure specifies the conditions for determining the nitrogen content of the feed according to Kjeldahl. The procedure for determining the nitrogen content is applicable to all levels in all feed types. Under the procedure nitrogen in nitrites, nitrites, azo or hydrazine compounds shall not be determined.
After mineralisation of the sample with hot sulphuric acid in the presence of a catalyst, displace ammonia with sodium hydroxide. Nitrogen substances shall be determined by titration alkalimetric (acidimetric).
Repeatability
The difference between two parallel determinations carried out on the same sample shall not exceed:
| do 200 g/kg | 2 g/kg |
| od 201 g/kg do 400 g/kg | 1 %relat. |
| nad 400 g/kg | 4 g/kg |
Reproducibility
The difference between the two test results of the same sample carried out in two laboratories shall not exceed:
| do 160 g/kg | 4 g/kg |
| od 160 do 320 g/kg | 2,5 % relat. |
| nad 320 g/kg | 8 g/kg. |
2.2. Determination of the nitrogen content of the pepsin solution soluble in hydrochloric acid
Purpose, scope and principle
The procedure specifies the conditions for determining the nitrogen content of nitrogenous substances soluble by the pepsin solution in hydrochloric acid in feed. The procedure for determination shall apply to all contents and to all types of feed, with the exception of feed with additive urea and mineral feed.
The nitrogen content of pepsin soluble in hydrochloric acid is determined after 48 hours incubation of the Pepsin sample at 40 ° C by the Kjeldahl method.
Repeatability
The difference between the two parallel determinations carried out on the same sample shall not exceed, with the nitrogen content soluble by the pepsin solution in hydrochloric acid:
| do 200 g/kg | 4 g/kg |
| od 201 do 400 g/kg | 2 % relat. |
| nad 400 g/kg | 8 g/kg |
Reproducibility
The difference between two test results of the same sample carried out in two laboratories shall not exceed 2% of relays.
2.3. Determination of protein content
Purpose, scope and principle
The procedure specifies the conditions for determining the protein content of feed and is applicable to all feed of organic origin.
The protein content shall be determined by the method according to Barnstein after separation from the nitrogen matter of non-white origin by precipitating copper salts.
Repeatability
Not fixed.
Reproducibility
Not fixed.
2.4. Determination of amino acid content
Purpose, scope principle
The procedure specifies the conditions for determining the free content of all amino acids in feed on the amino acid analyser. The method does not make it possible to distinguish D and L forms nor amino acid salts.
Free amino acids are extracted with dilute hydrochloric acid. The total amino acid content shall be determined in an oxidised or non-oxidised sample after acidic hydrolysis by separation on an ionoxic column and subsequent reaction with a ninhydrin agent photometric at 570 nm. After oxidation of the sample, the amino acids cysteine and methionine are determined, without oxidation tyrosine and other amino acids (glycine, alanine, serine, threonine, valine, isoleucine, leucine, lysine, arginine, aspartic acid, glutamic acid, phenylalanine, histidine and proline) may be determined in both oxidised and non-oxidised samples.
Repeatability
Repeatability values for different amino acids and different feedingstuffs are part of the complete version of the method.
Reproducibility
Reproducibility values for different amino acids and different feedingstuffs are part of the complete wording of the method.
2.5. Determination of urea content
Purpose, scope and principle
The procedure specifies the conditions for determining the urea content of feed with additive content of that substance.
Urea is determined, after the water leaching of the sample by Carres reagents, by reaction with p-dimethylaminobenzaldehyde spectophotometric at a wavelength of 420 nm.
Repeatability
Not fixed.
Reproducibility
The difference between the two test results of the same sample carried out in two laboratories shall not exceed:
| od 2 do 20 g/kg | 2 g/kg |
| od 20 do 100 g/kg | 10 % relat. |
| od 100 do 200 g/kg | 10 g/kg |
| nad 200 g/kg | 5 % relat. |
2.6. Determination of ammonia content in fish meal
Purpose, scope and principle
The procedure specifies the conditions for determining the ammonia content of fish meal. It is applicable to ammonia content expressed as NH3 up to 2,500 mg / kg.
The ammonia from the sample shall be extracted into the water leaching, dissipated with magnesium oxide and determined by titration alkalimetric (acidimetric).
Repeatability
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Regulation Information
| Citation | Decree of the Ministry of Agriculture No. 16 / 2000 Coll., amending Decree of the Ministry of Agriculture No. 222 / 1996 Coll., laying down the methods of sampling, the methods of analysis of feed, additives and premixtures and the method of storage of samples subject to destruction |
|---|---|
| Regulation Type | - |
| Author | - |
| Collection | Code of Laws |
| Date of Promulgation | 11.02.2000 |
|---|---|
| Effective from | 11.04.2000 |
| Effective until | - |
| Status | Valid |
The regulation text is for informational purposes only.
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