Decree No. 415 / 2009 Coll.
Ordonnance on the establishment of sampling requirements and the method of publication of methods of analysis of products for feeding
Valid
Order
Effective from 01.12.2009
Text versions:
01.12.2009
30.11.2009
415
DECLARATION
of 19 November 2009
laying down the requirements for sampling and the method of publication of methods of analysis of products for feeding
The Ministry of Agriculture provides for the Act No. 91 / 1996 Coll., on Feed, as amended by Act No. 244 / 2000 Coll., Act No. 147 / 2002 Coll. and Act No. 214 / 2007 Coll.:
(1) This decree implements the relevant regulation of the European Community1) and regulates, following the directly applicable regulation of the European Community2)
(a) the sampling requirements; and
(b) the method of publication of the methods of analysis of the products for feeding.
(2) This decree is without prejudice to the sampling procedures and the frequency of sampling provided for by other legislationm3).
Samples intended for official control of pesticide residues in feed products shall be taken and processed in accordance with the procedure set out in the Annex to this Regulation.
The publication of the methods of analysis of the products to feed (4) shall be done in a way that allows remote access by the Ministry of Agriculture.
Transitional provision
Samples taken before the date of entry into force of this Order shall be assessed in accordance with existing legislation.
Repeal
The following shall be deleted:
1. Decree of the Ministry of Agriculture No. 124 / 2001 Coll., laying down the requirements for sampling and the principles of methods of analysis of feed, additives and premixtures and the method of storage of samples.
2. Decree No. 497 / 2004 Coll., amending Decree No. 124 / 2001 of the Ministry of Agriculture Coll., laying down the requirements for sampling and the principles of methods of analysis of feed, additives and premixtures and the method of storage of samples.
3. Decree No. 85 / 2006 Coll., amending Decree No. 124 / 2001 of the Ministry of Agriculture Coll., laying down the requirements for sampling and the principles of methods of analysis of feed, additives and premixtures and the method of storage of samples, as amended by Decree No. 497 / 2004 Coll.
Efficacy
This Decree shall take effect on 1 December 2009.
Minister:
Ing. Shebesta v. r.
Annex to Decree No 415 / 2009 Coll.
Procedure for the collection and processing of samples intended for official control of pesticide residues in feed products
Terms
(a) Sampling is a procedure used to collect and create a sample.
(b) Sample devices are tools such as a blade, knife or needle to take a partial sample from a bulk material or piece of material too large to be used as a partial sample, as well as sample dividers used to prepare a laboratory sample from an aggregate sample or to prepare a test dose from a test sample and a specific sampling device as described in ISO and IDF1 standards). For materials such as grazing, the hand of the collector may be considered as a sampling device.
(c) The person authorised to take samples shall be the person trained in the sampling procedures and, where appropriate, authorised by the sampling institute and shall be responsible for the whole procedure including the preparation, packaging and dispatch of the laboratory sample. It shall comply with the sampling procedures laid down, lead to complete documentation of samples and cooperate closely with the laboratory.
(d) The sample is a part of the material taken from a larger quantity of material. The sample is representative of the lot, aggregate sample, etc., as regards the pesticide residue content and not necessarily from the perspective of other characteristics.
(e) The size of the sample is the quantity of the material which constitutes the sample.
(f) The lot is the quantity of feed which, according to the collector, has uniform characteristics such as origin, producer, type, packing plant, type of packaging, etc. The suspected lot is a lot where, for whatever reason, there is a suspicion that it contains excess pesticide residues.
(g) The incremental sample shall be the quantity taken from one random place in the lot.
(h) The aggregate sample shall be the whole resulting from the merger and the careful mixing of sufficiently large incremental samples taken from the lot.
(i) The laboratory sample shall be a representative quantity of material taken from the aggregate sample and sent to the laboratory or, where appropriate, the aggregate sample or part thereof.
j) The test sample is a material separated from the laboratory sample for analysis and treated with subsequent mixing, crushing, dilution, etc., allowing the removal of test doses with the smallest possible sampling error.
(k) The test dose is a representative quantity of materials taken from the test sample which is sufficient to determine the concentration of pesticide residues.
Explanatory note:
1) International standard ISO: Cereals - sampling (grain), International standard ISO: Packed leguminous - sampling, International standard ISO: Sampling - tea, International standard IDF: Milk and milk products - sampling methods.
1. Sampling
(1) Each lot must be sampled separately. If more samples are taken from the lot, the incremental samples should be represented in the aggregate sample by approximately the same proportion.
(2) The consignment may consist of one or more lots. The lot may be mixed, for example due to sorting or production process. Where a consignment of lots is composed of different operators, each lot shall be assessed separately. Where the boundaries or size of individual lots are not clearly defined for a large consignment, each of the series of wagons, lorries or cargo spaces in the ship may be considered a separate lot.
(3) Sampling equipment may be used for sampling. The incremental samples shall be taken from a randomly selected place, unless physically possible, from a randomly selected place in the accessible part of the lot. Where partial samples are taken several times during loading or unloading of the lot, the "place 'of sampling shall mean the time. The incremental samples shall contain sufficient material to produce a laboratory sample and shall be carried out in such a way as to avoid contamination or damage to the samples which could affect the results of the analysis.
(4) The minimum number of incremental samples taken from the batch for the determination of pesticide residues shall be as follows:
| Volně ložená nebo balená krmiva, dá se předpokládat, že jsou dobře promísena nebo homogenní | Volně ložená nebo balená krmiva, která nemusí být dobře promísena nebo homogenní | ||||||
|---|---|---|---|---|---|---|---|
| Hmotnost partie | Počet obalů v partii | ||||||
| Do 50 kg | 50-500 kg | > 500 kg | 1-25 | 26-100 | > 100 | ||
| Počet dílčích vzorků | 1 | 3 | 5 | 10 | 1 | 5 | 10 |
(5) In particular, grains, oil seeds, premixtures, compound feed and feed materials of a free-form nature, chequered cake and extracted scrap are to be considered as feed products which are expected to be well mixed or homogeneous, etc. In particular, granulated products for feeding, whole grains, cake and extracted scrap in the original state, bulk feed, etc.
(6) The incremental samples shall each consist of one aggregate sample by combination and proper mixing. If it is not possible to create an aggregate sample by mixing, the following alternative procedure may be followed. If by mixing or dividing the aggregate sample material may be damaged (and thus affect the residue content), or if by mixing the material cannot achieve a more uniform distribution of residues and more representative laboratory samples, the material shall be randomly distributed between duplicate laboratory samples when subsamples are taken. In this case, the average of the valid results obtained from the laboratory samples analysed shall be used as a result.
(7) The incremental samples shall be large enough to allow all laboratory samples to be taken from the aggregate sample. Where individual laboratory samples are prepared for the sampling of the incremental sample, the sum of the laboratory samples shall be considered as the aggregate sample at the time of sampling from the lot.
(8) Description of incremental samples and minimum size of laboratory samples:
| Klasifikace produktu | Forma dílčího vzorku, který má být odebrán | Min. velikost laboratorního vzorku |
|---|---|---|
| Obiloviny a luštěniny | balení nebo materiál odebraný vzorkovacím zařízením | 1 kg |
| Hlízy a kořeny (např. brambory, řepa) o hmotnosti 25-250 g | celé kusy | 1 kg (nejméně 10 ks) |
| Hlízy a kořeny o hmotnosti nad 250 g | celé kusy | 2 kg (nejméně 5 ks) |
| Volně ložený živočišný tuk | materiál odebraný vzorkovacím zařízením alespoň ze tří míst | 0,5 kg |
| Tekuté produkty (např. mléko, rostlinné oleje) | balení nebo materiál odebraný vzorkovacím zařízením | 0,5 l nebo 0,5 kg |
| Ostatní | balení nebo materiál odebraný vzorkovacím zařízením | 0,5 kg |
| balení nebo materiál odebraný vzorkovacím zařízením | 0,5 kg | |
| Doplňkové látky a premixy | balení nebo materiál odebraný vzorkovacím zařízením | 0,2 kg |
2. Sampling Protocol
The sampling officer shall record the nature and origin of the lot, the name of the owner, supplier or transporter, the date and place of sampling and any other relevant information. Any deviation from the recommended sampling method shall be recorded. One signed copy of the report shall accompany each duplicate sample and one copy shall be retained by the authorised official. One copy of the sampling protocol shall be received by the owner of the lot or his representative, whether they are to receive a laboratory sample. Where sampling protocols are made in electronic form, they shall be sent to the same addressees and a verifiable copy shall be kept.
1. Preparation of a laboratory sample
If the aggregate sample is greater than necessary for the production of the laboratory sample, it shall be divided to form a representative part. Sampling equipment, quarters or other appropriate method of reducing the sample may be used, but fresh plant products shall not be cut or cut. If necessary, duplicate laboratory samples shall be taken or prepared at this stage according to the procedure described above.
2. Packaging and transport of laboratory samples
The laboratory sample shall be stored in a clean inert container which ensures adequate protection against contamination, damage or leakage of the sample. The container shall be sealed, securely marked and accompanied by a sampling report. If bar code is used, alphanumeric information is also recommended. The sample shall be delivered to the laboratory as soon as possible. During transport, the sample must not be degraded (e.g. fresh samples must be kept cool).
3. Preparation of the test sample
A specific code shall be assigned to the laboratory sample, which shall be entered in the sampling report together with the date of arrival of the sample and the size of the sample. The part of the product to be analysed 2), i.e. the test sample, must be separated as soon as possible.
4. Preparation and storage of the test dose
The test sample shall be diluted and well mixed as necessary in order to remove representative test doses. The size of the test doses is determined by the analytical method and the effectiveness of the mixing. The dilution and mixing methods shall be recorded and shall not affect the residues present in the test sample. If necessary, the test sample shall be processed under specific conditions, e.g. at a temperature below 0 ° C to minimise adverse effects. If processing could adversely affect residues and if available alternative procedures are available, the test dose may consist of whole pieces or parts taken from whole pieces. It is likely that such a test dose, consisting of a small number of incremental samples or parts, is not very representative of the test sample and therefore a sufficient number of duplicate test doses should be analysed to determine the degree of uncertainty of the mean value. If the test doses are to be stored before analysis, the method and duration of storage should not affect the quantity of residues present. For repeated or confirmatory analysis, additional test doses shall be taken as appropriate.
5. Criteria for checking compliance
The results of the analysis shall be obtained from one or more laboratory samples taken from the lot and obtained in a state eligible for analysis. The results shall be supported by acceptable quality control data (3). If a residue is found to exceed the MRL (MRL), it is necessary to confirm its identity and verify the concentration by analysing one or more additional test doses obtained from the original laboratory sample. The MRL applies to the aggregate sample.
The batch meets the MRL if the result or results of the analysis do not exceed that MRL.
If the results for the aggregate sample exceed the MRLs, the following shall be taken into account when deciding to reject the lot:
(a) results obtained from one or more laboratory samples; and
(b) the accuracy and accuracy of the analysis resulting from the quality control supporting data.
Explanatory notes:
(2) Regulation (EC) No 396 / 2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91 / 414 / EEC.
3) Quality management procedures for pesticide residue analysis. SANCO / 3103 / 2000; the changes can be found on the Commission website.
1) Commission Directive 2002 / 63 / EC of 11 July 2002 laying down Community methods of sampling for the official control of pesticide residues in and on products of plant and animal origin and repealing Directive 79 / 700 / EEC.
2) Article 7 and 11 of Regulation (EC) No 882 / 2004 of the European Parliament and of the Council of 29 April 2004 on official controls performed to ensure the verification of compliance with feed and food law, animal health and animal welfare rules.
(3) Annexes 1 and 3 to Decree No 291 / 2003 Coll., concerning the prohibition on the administration of certain substances to animals whose products are intended for human consumption and on the monitoring (monitoring) of the presence of unauthorised substances, residues and contaminants for which animal products could be harmful to human health, animal health and their products, as amended.
4) Article 11 of Regulation (EC) No 882 / 2004 of the European Parliament and of the Council. Commission Regulation (EC) No 152 / 2009 of 27 January 2009 laying down methods of sampling and analysis for the official control of feedingstuffs. Commission Regulation (EC) No 121 / 2008 of 11 February 2008 laying down a method of analysis for determining the starch content of products used in animal nutrition.
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Regulation Information
| Citation | Decree No. 415 / 2009 Coll., laying down the requirements for sampling and the method of publication of methods of analysis of products for feeding |
|---|---|
| Regulation Type | Order |
| Author | - |
| Collection | Code of Laws |
| Date of Promulgation | 30.11.2009 |
|---|---|
| Effective from | 01.12.2009 |
| Effective until | - |
| Status | Valid |
The regulation text is for informational purposes only.
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